# US Environmental Protection Agency — Hazardous Materials Safety Interpretation

- **operation:** document
- **citation:** 00-0308
- **title:** US Environmental Protection Agency — Hazardous Materials Safety Interpretation
- **source type:** guidance
- **agency:** Pipeline and Hazardous Materials Safety Administration
- **status:** guidance
- **official:** true
- **published on:** 2000-12-04
- **effective on:** Not available
- **summary:** 00-0308 response to US Environmental Protection Agency concerning 172.101.
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- **app url:** https://regulus.evalyn.ai/document/phmsa-interpretation-00-0308
- **source url:** https://www.phmsa.dot.gov/sites/phmsa.dot.gov/files/legacy/interpretations/Interpretation%20Files/2000/000308.pdf
**body:**

<<<PAGE 1>>>

U.S. Department
of Transportation
40ven Street, SW
Washington. D.C.
20590
Research and
Administration
Special Programs
DEC - 4 2000
Mr. David Friedman
Ref. No. 00-0308
US Environmental Protection Agency
Office of Research and Development
Washington DC 20460
Dear Mr. Friedman:
This is in response to your letter dated August 22, 2000 regarding the shipment of environmental
samples. Specifically, you ask if a inside receptacle of a combination packaging that does not
meet the outage requirements of 49 CFR 173.24a(d) may be placed inside a secondary packaging
capable of containing all of the liquid in the primary receptacle.
Section 173.24a(d) states that liquids may not completely fill a receptacle at a temperature of
55 °C (131 F) or less. It is the opinion of this office that hazardous material may be placed in
an inside container of a combination packaging that does not itself meet the outage requirements
of § 173.24a(d) provided that the inner packaging is placed within a secondary inside packaging
which does meet the outage requirements and other applicable packaging requirements of the
Hazardous Materials Regulations (49 CFR Parts 171-180).
I hope this satisfies your request.
Sincerely,
Thomas G. Allan
Senior Transportation Regulations Specialist
Office of Hazardous Materials Standards

<<<PAGE 2>>>

Gale
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
WASHINGTON, D.G. 20460
8173.24
Packaging
00 - 0308
RESEARCH AND DEVELOPMENT
OFFICE OF
August 22, 2000
Mr. John Gale
Office of Hazardous Materials Technology (DHM-21)
Research and Special Programs Administration
U.S. Department of Transportation
400 Seventh Street, SW
Washington, DC 20590-0001
Dear Mr. Gale,
I am writing to follow up on our recent meeting concerning the Department of
Transportation's (DOT) requirements with respect to the shipment of environmental samples that
are to be analyzed for either purgable organic compounds or mercury.
In order to prevent analyte loss, it is important that the vials containing the samples of
water be completely filled. To ensure that they are filled, the Environmental Protection Agency
(EPA) has issued regulations that specify that the samples vials not contain any free headspace or
outage. The confusion relates to the apparent contradiction between the EPA and the DOT
regulations in 49 CFR 173.4(a)(2)(i) and 49 CFR 173.24(a)(d) which specify that containers may
not be completely filled with liquid (i.e., requires headspace).
Since the DOT regulations are designed to prevent loss of sample in the event the
container holding the liquid breaks, it is our understanding that if the sample vial was itself
packaged in a sealed container that meets the outage requirements and which would contain all
the liquid in the event the inner vial ruptured, then the secondary inner receptacle's outage would
meet the definition of an acceptable container and the combination would comply with the outage
provisions of the Hazardous Materials Regulations.
I would appreciate your confirming our understanding of the DOT regulations. If you
have any questions about the information in this letter, do not hesitate to contact me at:
(202) 564-6662 or at friedman. david@epa.gov. Thank you for the guidance you already have
provided. I look forward to receiving your response.
Sincerely yours,
wit Tristman
David Friedman
Recycled/Recyclablo.• Printed with Vegetable Oil Based inks on 100% Recyced Paper (40% Postconsumer)
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