# Hercules Incorporated — Hazardous Materials Safety Interpretation

- **operation:** document
- **citation:** 98-0609
- **title:** Hercules Incorporated — Hazardous Materials Safety Interpretation
- **source type:** guidance
- **agency:** Pipeline and Hazardous Materials Safety Administration
- **status:** guidance
- **official:** true
- **published on:** 1998-04-23
- **effective on:** Not available
- **summary:** 98-0609 response to Hercules Incorporated concerning 178.814.
- **machine formats:** - **json:** https://regulus.evalyn.ai/document/phmsa-interpretation-98-0609.json
- **markdown:** https://regulus.evalyn.ai/document/phmsa-interpretation-98-0609.md
- **app url:** https://regulus.evalyn.ai/document/phmsa-interpretation-98-0609
- **source url:** https://www.phmsa.dot.gov/sites/phmsa.dot.gov/files/legacy/interpretations/Interpretation%20Files/1998/980609.pdf
**body:**

<<<PAGE 1>>>

U.S. Department
of Transportation
Research and
20590
Special Programs
Administration
APR 2 3 1998
Mr. I.L. Kerstetter
Hercules Incorporated
Hercules Plaza
1313 North Market Street
Wilmington, DE
19894-0001
-
Dear Mr. Kerstetter:
This is in response to your January 12, 1998 letter and
subsequent telephone conversations with Mr. Ryan Posten of my
~ pressure relief devices and vented closures on metal intermediate
- bulk containers (IBC) be removed and their apertures plugged or
rendered inoperative.
(lid) on an IBC is designed to function as a non-reclosing
Specifically, you stated if a closure
20 psig rupture diso may be replaced with a rupture disc that has
pressure relief device with a burst pressure of 20 psig, then the
a minimum burst pressure of 29 psig when conducting the
hydrostatic pressure test.
Your understanding of this requirement is not correct.. You may
pressure relief device.
not replace the non-reclosing pressure relief device with another
relief devices (PRD) and vented closures must be removed and
Section 178.814 (b) states all pressure
their apertures
the hydrostatic pressure test on the IBC.
(openings) plugged or rendered inoperative during
aperture may be held in place by threading, bolting, welding,
The plug closing the
clamping or other suitable means.
burst pressure of a pressure relief device is required to be
Additionally, you asked if the
marked on the container or on the closure of a (metal) IBC. The
answer is
no.
If you have
contact us.
any further questions, please do not hesitate to
sincerely,
Director, Office of Hazardous
Materials Standards

<<<PAGE 2>>>

Posten
Fele: 178.814
•HERCULES
SC: 322, 3602
Hercules Plaza
Hercules Incorporated
Wilmington, DE 19894-0001
1313 North Market Street
(302) 594-5000
Mr. Edward Mazzullo
Director (DHM-10)
January 12, 1998
• Office of Hazardous Materials Standards
Office of Hazardous Materials Safety
Research & Special Programs Administration
400 Seventh Street NW
U.S. Department of Transportation
Washington, D.C. 20590
Dear Mr. Mazzullo:
HYDROSTATIC PRESSURE TEST
Hercules' is requesting clarification of the qualification test required by 49
:
CFR 178.814 for 31A metal intermediate bulk containers.
49 CFR 178.814(d) requires a hydrostatic pressure test of 200 kPa (29 PSIG)
for at least 10 minutes. 49 CFR 178.814(b) states that all pressure relief devices and
vented closures must be removed and their apertures plugged or rendered inoperative.
If the closure (lid) on an IBC is designed to function as a non-reclosing
pressure reliet device with a burst pressure of 20 PSIG, then per 49 CFR 178.814(b)
the 20 PSIG rupture disc may be replaced with a rupture disc that has a minimum
burst pressure of 29 PSIG when conducting the hydrostatic pressure test.
Please advise if Hercules' interpreiation of this regulation is correct. Also,
must the 20 PSIG burst pressure be marked on the container and/or closure?
Thank you for your time and cooperation.
Very truly yours,
elteratetter
L. L. Kerstetter
Regulations
LLK:ims
Purchasing & Transportation
...

<<<PAGE 3>>>

H.
B. LUFFY 1VL.
10 1 _
P.10111
FAX
abDuit,
SINCE 1951
ANDREW B. DUFFY, INC.
PH
(609) 845-4900
P.O. BOX #UC0
FAX (609) 845-3921
CROWN POINI ROAD
THOROFARE, NI WANKSFY
PATE: 2/6/98
TO: Mr. RUN POSTIN
AT: DOT/STOS DIVISION
PHONE#. 708 - 76A - 8,553
FAX#: 702 366 3753
FROM: Lizar in CeLi
NO. PAGES:. I/ii...
Mr. POSTINE.
INCORPORATED, LAM ENCLOSING THE FOLLOWINGi.
• INFORMATION ON EMERGENCY VENT LIN, CLAR
WÜHETCH WHOWING FIXTURE USED FOR HYDROSTATIS
TESTING (174, 514(6)) (1P8)
CONE DA DUE TEST REPORTS FROM 1997- 123(-J
1 MODE THIS NEURMATUR LI HELPED DIRE
BRIAN DUiL
FX 302 594 7304
Manuf. Suffy) Drawings

<<<PAGE 4>>>

A. B. DUFFY INC.
TEL: 609-845-3921
Feb 06 98
11:56 No.004 P.02
ANDEW B. DUrY, INC.
569 P.O. Boxf, Crowu Polit Road
Thorofare, NJ 08086
Ps, 2/1!.
abDuffy
Custom Mcral Fabrication
Since 1957
(68)9)845490
Fax: (609) 815-3921
(215) 922-4909
EMERGENCY
VENT LID
WITH RIEKE FITTING.
0.060"
(4) "bmpees"
)
304 Ss (6º840)
CÜMLOSUN LID
RIEKE "SAFETY
ELUSURE " IN CTR
PLAN
2334" NOM —
ScALr:
OD
/É "=/'o"
ELEVATION
ELAMP RING : Y8" THR. 304 SS
LUAS ON RING - 9/16" THK.
ONE GUa WITH BI4"Ø HUnE
ONE AVI- TAPPED F/RR' UNC.
BOLT. - 304 5$ 9/16" UNC X4"L. HExA)
WIThe 9l16" UNC HEX NUT. S/S,
KMA" 81i7-8/prs

<<<PAGE 5>>>

A:
B. DUFFY INC.
TEL: 609-845-3921
Feb 06 98
11:57 No. 004 P.03
ANBREW B. DUPPY, INC.
Bg 3/11
5 69 PO. Boxe, Crown Point Roas
•.:•
Thorofase, N) 08086
•
abDuffy
Custom Acta Nahricarion
Since 19S1
(609) 845-4900
Fax: (609) 845-3921
(215) 922-1909)
5" THR. 304 55
DISHED MEAD I
FOR TEST.
/BC.7: 10)
01.) 17C
VENTELOSURE iNOPERATIVE (PEr 178.814 (b))
FOR HYDROSTATIC TEST
5K- "B"
BMD
2/6/88
....

<<<PAGE 6>>>

A.
B. DUFFY INC.
TEL: 509-845-3921
Feb 05 98
11:57 No. 004 P.04
liar
Да 4!!.
..
• PACKAGE KLULAKCH LABORATORY
ROCKAWAY, NEW JERSEY 07866
Job No.: L-5038
Date Tested: 6/6/97
LABORATORY DOT VIBRATION TEST
ON A
46" DIAMETER. STEEL TANKIBC
PERFORMED OR:
Andrew B. Duffy, Inc.
Crown Print Rnad
P.O. Box #1
... i i. 137
Thorofare, Nu 08086
MATERIAL TESTED:
follows:
One 46" diameter steel portable tank/IBC filled with sand is briefly described as
Identification:
46" diameter steel portable tank/IBC
Oulside Dimensions:
48-1/4" × 46" × 79-3/8"
Gross Weight:
5,747 Ibs.
Manufactured by:
Andrew B. Duffy, Inc.
Contents:
Lead weight and 3,739 Ibs. of water
NOTE: This report is intended solely for the informational purposes of the addrasste.
Package Rescarch Laboratory makes no representation or warranty, expressed or
implied, of any kind or nature, to the addressee or any third persons, as to the product
involved, its general merchantability or its suitability for any particular purpose.

<<<PAGE 7>>>

A. B. DUFFY INC.
TEL: 509-845-3921
Feb 06 98
11:58 No.004 P.05
MATERIAL TESTED: (Continued)
Page 2
Photo No.: L-5038-A
Tank/IBC filled and ready for testing.
Photo No.: L-5038-B
Method of performing Vibration Test
IEST PROCEDURES:
The vibration test was performed on a filled Metal Portable Tank/IBC as specified
in 49 Code of Federal Regulations 178.819 Paragraph 178.819 (b) (1), (2), (3), & (c).
Vibration Test
Equipment: A 10,000 Ib. capacity variable speed drive synchronous
motion L.A.B. vibration package tester with a circular
motion at 1" double amplitude.
The metal portable tank/IBC, filled with sand was placed on the table of the
vibration tester. A steel "" beam was placed on the vibration table to prevent the
tank/IBC from falling over, but the tank/IBC was allowed room to move vertically and
aused the tank/IBC to leave the testing table momentarily during each cycle. A fla
ounce. The test was performed for one hour at 205 pm. Vibration at this spee
metal shim was passed between the bottom of the tank/IBC and the table while al that
vibration speed.
-

<<<PAGE 8>>>

A. B. DUFFY INC.
TEL: 609-845-3921
Feb 06 98
11:59 No.004 P.05
Pa. 6/11
Page 3
TEST RESULTS:
"!''
Photo No.: L-5038-C&D
Condition of the metal portable tank/IBC
after the Vibration Test
Bryan Berg
SENIOR PACKAGING TECHNICIAN

<<<PAGE 9>>>

П ПІГГУ ThIr
ТГ 000 0AE T071
17 00 0 00a d
*
Pr.?/1
VIBRATION TEST
(b) Test Method (1) A sample IBC, sclecied at random, must be filled and closed as for shipment.
(Z) The sample DBC must bu placed on a vibrating platform that has a vertical double amplitude
(peak to poak displacement) of 1 inch. The IBC must be constrained horizontally 1o prevent it
1) hales misbe pellomed or or bur ate tequency that also the package a to raised
(0.063 inch) thickness (such as stec strapping or puparbuald) car ho pagned between the bottom
pa. to least equally effective may be used.
Icalage.
SHE TEST REPORT OF PACKAGE RESEARCH LABORATORIES.
-
Peeranned By aBove 6l5/97

<<<PAGE 10>>>

B. DUFFY INC.
TEL: 609-845-3921
Feb
06 98
12:00 No.004 P.08
Pa 8/11
BOTTOM LIFT TEST
178.811
(b) Special prepatation for the bottosh lift tost. The intermediate bulk container must be loadcd to
1.25 times its maximum pormissible gross mass, the load boing evonly distributed. (c) Tost
method. All intermediate bulk container design types must be raised and lowered twice by a litt
truck with the forks contrally positioned and spaced at thrac quariors of the dincasion of the side
dreyfund the points of ontry are fixed). The fonks mus ponstrate to throo quartom of the
RATIN GROSS MASS:
WT. OF CONTAINER TESTED
EMPTY IBC
1130LB.
WT. OF WATER
(PER P.R. LABS)
3769 .R.
ADD FOR 1.1 S.G.
(PER P.R 1.ARS)
TOTAL REQ'D GROSS
377 1B.
5276 T.B.
-
DESIRED RATED GROSS MASS
REQUIRID TEST FACTOR 1.25
5300LB.
REQUIRED TEST WI.
× 1,25
6625LB.
TARE
LEAD WEIGHT
1130LB.
CONTENTS
758LB.
800/6s
3769LB.
DISK #1 (2.5 X .32"D))
569 TR
193K #2 (2.23 × 34"»,
l0Is. 1b5t Wl.
6676LB.
4JU AP.
OUR TEST METHOD:
6650163
1. ADI LEAD WEIGITS
3. INSTALL COVER AND RING
1. PLACE DISKE ON TOP
5. MARK FORKS AT 36" FROM END (3/4 OF 48")
6. APPROACII UNIT, INSERT FORKS TO MÄRKS
7. LIFT 4 FRET FROM FLOOR
8. LOWER TO FLOOR AND REPEAT
9. REPEAT STEPS 6, 7,8 ON OTHER SIDE
TEST IMPI FTEN DATE:
DULUMENTALIUN: VIDEO VOTI
(/70/97
BY:
I.SJGN TYPI: J3C' 1
PHOTO.

<<<PAGE 11>>>

"
A. B. DUFFY INC.
TEL: 609-845-3921
Feb 06 98
12:01 No.004 P.09
P4.1 1/11
•
LEAK PROOFNESS TEST
IBC, 178.813
(1) General. The leakproofness lust must be conducted for the qualification of all IBC
design lypos and on all production units intended to contain liquids or inlended to conlain solids
that are loaded or discharged under pressurc.
(b) Special preparation for the leakproofness lest. Vented closurcs must either be
replaced by similar non-vented closuras or the vent must bo scaled. For mclal 13C design lypes,
the initial test must carried out bofore the fitting of any thermal insulation equipment.
178.801(l).
(d) Criteria for passing the fest. .... there may be no lcakage of sir from the IBC.
OUR TEST METHOD
1. Use same method as periodic air test.
TEST COMPLETED DATE:
5/21/42 BY:
DESIGN TYPE: IC 1
....
.mu. .

<<<PAGE 12>>>

A. B. DUFFY INC.
TEL: 609-845-3921
Feb 06 98
12:02 No.004 P.10
Pa. 10/11
HYDROSTATIC PRESSURE TEST
BC, 178.814
(a) General. The hydrostatic pressure test must be conducted for the qualifications of all
melal... TBC: desien typos intended to contain liquids or intended to contain solids loaded of
(b) special preparadon for the hydrostailo prossure desi. Bus metal BBC'» the lest aust le
carried out before the fitting of any thermal insulation equipmont. For all IBC's, pressure relie!
devices and vented closures must be removed and their apertures plugged or rendered inopcrative.
(c) Test mothod. Hydrostatic gauge pressure must be measured al the lop of the ISC.
The lost must be carried oul for a period of al loast 10 nunutes applying a hydrostatic gauge
pressure not less than that indicated in paragraph (d) of this section. The JIC may not he
mechanically restrained during the rest.
(d) Hydrostatic gauge pressure applicd. (1) For motal IBC: design type 31A,...9.4 psig.
(2) l'or mela) IC design type 31A...29 psig. For metal IBC design types...31 A, the rests
in paragraphs (dI) and (d)(2) of this paragraph must be conducted consecutively.
(3) For motal IBC design types 21A.., for packing group I solids, 36 psig gauge pressure.
(c) Criteria for passing the test. (1) For metal IBC's, subjected to the 9.4 psig test
pressurc specified in paragraph (d))) of this section, there may be no leakage or permanont
doformation that would make the IBC unsafe for transportation.
(2) l'ol melal I. & intended to contain hquids, when subjocted to the 29 psig ..... lus/
pressuro, spocified in paragraphs (d)(2) and (d)(3) of this section, respoctively, there may bo no
leakage.
TesT to BalsiG
6/20/97
Perporaro by Mike Krogen
Vidio: yes
.....
.....
1aia aos..
...
-
• .
man.

<<<PAGE 13>>>

A. B. DUFFY INC.
TEL: 609-845-3921
Feb 06 98
12:03 No.004 P.11
Pa.
"/,,
DROP TEST
IBC. & DOT S7
DOT 57,178.253-5 Testing
(a)....the tank must be filled with a liquid 1o not loss than the rated gross weight.
(2) Drop Test. 'Tho lank must be capable of withstanding, without Icakage ol'contents a
2-foul fice deup ulito a flat unyiolding horizontal surface, kiriking the tangel surface in the position
and antitudc from which maximum damage to the tank (including piping and fittings) is expected.
TBC, 178.810 Drop Tost
(n) Gunusal The drop lost must he conduadd for the qualification orall BC dosio ropes
and performed poriodically as specitied in 178 801(c) of Mis sulpal,
(b) Special preparallon for the drop tesl, (1) Metal, ...IC's intended in contain coral
solids must be filled to not loss than 95 percont of their capacity, or if intended to contain liquids,
to not less than 98 perconi of die wapavily. Pressure relict dovioos must by romoved and their
aportures plugged or rendered inoperative.
(c) Test Mcthod. Sainples of all IBC design types must be dropped onto a rigid, non
resilient, smooth, tlat and horizontal surface. The point of impact must he the most vulnerable
part of the base of the IBC being tested. Following the drop, the IBC must be restored to the
upright position for obscrvation.
(d) Drop height. (1) for all IBC"s, drop heights are specified as follows:
(i) Packing Group I 5.9 Ft.
(i) Packing Group I! 3.9 Ht.
(2) Drop tests are to be performed with the anlid or liquid to be transported or with a non-
hazardous material having essentially the same physical charactcristics.
(3) The spocific gravily and viscosity of a substituted non-hazardous matcrial used in the
drop test for liquids must be similar to the hazardous material intended for transportation. Water
may also be used for the drop test under the following conditions.
(c) Criteria for passing the tes!. For all IBC design types there may be no loss of contents.
...
provided that no further leakage occurs. ...
: 1997
"Pro: ye.
.....
.•. . ...

<<<PAGE 14>>>

HER. 248 REV. 10-94
•HERCULES
JAN 13'93
FIRST C
MR EDWARD MAZZULLO
DIRECTOR (DHM-10)
OFFICE OF HAZARDOUS
OFFICE OF HAZARDOUS MATERIALS SAFETY
MATERIALS STANDARDS
RESEARCH & SPECIAL PROGRAMS
US DEPARTMENT OF TRANSPORTATION
ADMINISTRATION
WASHINGTON DC 20590
400 SEVENTH STREET NW
- **truncated:** false
- **body characters:** 14047
